矿物药芒硝中无机元素的ICP-MS分析
Study on inorganic elements of Natrii Sulfas by ICP-MS
分类号:
出版年·卷·期(页码):2013,33 (11):0-0
DOI:
10.16155/j.0254-1793.2017.01.01
-----摘要:-------------------------------------------------------------------------------------------
目的: 测定矿物药芒硝中无机元素的含量。方法: 采用电感耦合等离子体质谱(ICP-MS)法测定芒硝中的无机元素,并使用统计学软件SPSS 18.0对数据进行分析。结果: 测定了矿物药芒硝中的24种元素,除了Na元素外,Mg、K、Ca、Fe等元素的含量亦较高。另外,重金属及有害元素Pb、Cd、Cu、As亦有检出。建立了芒硝无机元素的指纹图谱。结论: 为矿物药芒硝的安全性评价及其质量标准的制定提供了科学的参考依据。
-----英文摘要:---------------------------------------------------------------------------------------
Objective: To determine the content of inorganic elements in Natrii Sulfas. Methods: The samples were determined by inductively coupled plasma-mass spectrometry (ICP-MS).The data was analyzed by the statistical software SPSS 18.0. Results: 24 elements were determined.In addition to the element Na,the contents of Mg,K,Ca,Fe were also high.Meanwhile,the heavy metals and harmful elements Pb,Cd,Cu,and As were also detected.The fingerprint chromatogram of inorganic elements in Natrii Sulfas was established.Conclusion: This study provides a scientific reference for the safety evaluation and establishment of quality standard of Natrii Sulfas.
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1 TAO Hong-jing (陶弘景).Ming Yi Bie Lu (edit and proofread version)[名医别录(辑校本)][M].Beijing (北京):People's Medical Publishing House (人民卫生出版社),1986.8
2 ChP(中国药典)[S].2010.Vol Ⅰ(一部):118
3 WU Yong-jun(吴拥军),LIU Jie(刘洁),WU Yu-ming (吴予明),et al.Determination of polysaccharide from Chinese medicine Morinda officinalis how and its trace elements analysis (中药巴戟天多糖的测定及其微量元素分析)[J].Spectrosc Spect Anal (光谱学与光谱分析),2005,25(12):2076
4 WANG Bin(王斌),TANG Zhi-shu(唐志书),ZHOU Yong-xue(周永学).Research and thinking on mineral Chinese herbal(矿物药类中药研究现状与思考) [J].J Shaanxi Coll Tradit Chin Med (陕西中医学院学报),2010,33(6):94
5 LU Hong(路红),MENG Fan-yu(孟凡余),LI Wei(李伟).Gypsum processing and clinical function analysis (石膏炮制及临床功用分析) [J].Lishizhen Med Mater Med Res (时珍国医国药),2000,11( 6):568
6 LIU Sheng-jin (刘圣金),WU Kang-de(吴康德),LIN Rui-chao(林瑞超),et al.ICP-MS analytical studies on inorganic elements of mineral Chinese Medicine chlorite lapis(矿物药青礞石无机元素的ICP-MS分析) [J].Chin J Pharm Anal (药物分析杂志),2010,30(11):2067
7 ChP(中国药典)[S].2010.Vol Ⅰ(一部):80
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