期刊名称:药物分析杂志 主管单位:中国科学技术协会 主办单位:中国药学会承办:中国食品药品检定研究院 主编:金少鸿 地址:北京天坛西里2号 邮政编码:100050 电话:010-67012819,67058427 电子邮箱:ywfx@nifdc.org.cn 国际标准刊号:ISSN 0254-1793 国内统一刊号:CN 11-2224/R 邮发代号:2-237
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X射线荧光元素分析技术测定明胶原料中的铬
Rapid detection on Cr in gelatin by X-ray fluorescence elemental analysis technology
单位(英文):1. National Institutes for Food and Drug Control, Beijing 100050, China; 2. Dongying Institute for Drug Control, Dongying 257091, China; 3. Zhejiang Institute for Food and Drug Control, Hangzhou 310004, China; 4. Shangdong Institute for Food and Drug Control, Jinan 250101, China; 5. Jiangxi Provincial Institute for Drug and Food Control, Nanchang 330029, China; 6. Heibei Institutes for Food and Drug Control, Shijiazhuang 050011, China
分类号:
出版年·卷·期(页码):2012,32 (7):0-0
DOI:
10.16155/j.0254-1793.2017.01.01
-----摘要:-------------------------------------------------------------------------------------------
目的: 建立X射线荧光元素分析技术快速检测明胶原料中铬的方法。 方法: X射线荧光元素分析仪,测试时间180 s,标准偏差1σ,采用模式:塑料模式,取样量约5 g,关闭厚度修正。 结果: 此方法的检出限为10 mg·kg-1,与原子吸收测试结果比较,结果基本吻合。 结论: 该方法简便快速,可用于快速测定明胶原料中的铬。
-----英文摘要:---------------------------------------------------------------------------------------
Objective: To establish a method for rapid detection of Cr elements in gelatin by X-ray fluorescence elemental technology. Methods: X-ray fluorescence elemental analyzer was adopted with following settings,test time: 180 s,standard deviation: 1σ,mode: plastic mode.The sample weights were around 5 g,and the thickness correction was turned off. Results: Under the above mentioned conditions,the detection limit was 10 mg·kg-1,Compared with AAS,the results was coincidence. Conclusions: The method is simple and rapid,which can be used for the rapid detection of Cr elements in gelatin.
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1 FENG Yu-chuan(冯豫川),ZHAO Qing(赵青),LU Xiao-hua(鲁晓华),et al.Chromium pollution and its control in leather-making industry(制革工业中铬污染及防治).J Southwest Nation Coll(西南民族学院学报),2001,27(1):64 2 LIU Zheng-hao(刘峥颢),ZHAO Zhi-lei(赵志磊),XIA Li-ya(夏立娅).et al.The investigation of chromium content of food additive gelatin and food added gelatin in the market(市场中食品添加剂明胶及添加明胶的食品中铬含量本底调查).Food Sci Technol(食品科技),2010,35(2):224 3 XIE Xiu-hong(谢秀红),LI Yong-qin(李勇勤),MAI Jian-ping(麦剑平).et al.Study on content of heavy metal in medical gelatin hard gapsule shells(药用明胶硬胶囊壳中重金属含量的研究).Pharm Today(今日药学),2010,20(01):28 4 Tsuyumoto I,Maruyama Y.X-ray fluorescence analysis of hexavalent chromium using Kβ satellite peak observed as counterpart of X-ray absorption nearedge structure preedge peak.Anal Chem,2011,83(19):7566 5 HE Zheng(贺峥),HUANG YA-qin(黄雅钦),SHI Shao-jun(石绍军),et al.Determination of micro chromium in edible gelatin by using wet digestion(湿法消解测定食用明胶中的微量铬).Chin J Anal Lab(分析实验室),2009,28(5):97 6 Aranda PR,Moyano S,Martinez LD,et al.Determination of trace chromium(VI)in drinking water using X-ray fluorescence spectrometry after solid-phase extraction.Anal Bioanal Chem,2010,398(2):1043 7 LUO Li-qiang(罗立强),ZHAN Xiu-chun(詹秀春),LI Guo-hui(李国会).X-ray Fluorescence Spectrometer(X射线荧光光谱仪).Beijing(北京):,Chemical Industry Press(化学工业出版社),2008 8 GUO Xi-hua(郭西华),GUAN Ying(关颖),YANG La-hu(杨腊虎).et al.Analysis the Anemarrhena asphodeloides of space flight breeding with XRF and PXRD(航天诱变育种第4代知母的XRF、PXRD分析). Chin J Pharm Anal(药物分析杂志),2008,28(12):2100 9 GUAN Ying(关颖),GUO Xi-hua(郭西华),YANG La-hu(杨腊虎).et al.Study on the identification of standard and false Ejiao by XRF and PXRD(真伪阿胶的X射线荧光分析及X射线衍射鉴别研究).Chin J Pharm Anal(药物分析杂志),2009,29(10):1658 10 GUAN Ying(关颖),DING Xi-feng(丁喜峰),WANG Wen-jing(王文静).et al.Study on the method of X-ray fluorescent analysis and X-ray diffraction of Flos Trollii(金莲花的X射线荧光分析及X射线衍射技术研究).Chin J Pharm Anal(药物分析杂志),2006,26(11):1623 11 LIU Dan-chi(刘丹赤).Comparative study on pretreatment of sample for the determination of Pb in cosmetics(化妆品铅含量测定的样品预处理方法比较研究).Stud Trace Elements Health(微量元素与健康研究),2006,23(6):46 12 LIN Guo-zhen(林国桢),DU Lin(杜琳),LI Ke(李科).Study on the examination of paint lead with a portable X-ray fluorescence analyzer(便携式X射线荧光分析仪用于现场油漆涂层铅含量检测的研究).Chin J Health Lab Technol(中国卫生检验杂志),2011,33(10):1324
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