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期刊名称:药物分析杂志
主管单位:中国科学技术协会
主办单位:中国药学会
承办:中国食品药品检定研究院
主编:金少鸿
地址:北京天坛西里2号
邮政编码:100050
电话:010-67012819,67058427
电子邮箱:ywfx@nifdc.org.cn
国际标准刊号:ISSN 0254-1793
国内统一刊号:CN 11-2224/R
邮发代号:2-237
 

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根据测量不确定度的评定和分析拟定水分测定管不同标称容量的允差

Propose on allowance of different nominal capacities of moisture measuring tubes based on evaluation and analysis of uncertainty of measurement results

分类号:
出版年·卷·期(页码):2014,34 (3):0-0
DOI: 10.16155/j.0254-1793.2017.01.01
-----摘要:-------------------------------------------------------------------------------------------

目的:拟定水分测定管不同标称容量的容量允差;方法:通过对甲苯法测水分不确定度评定和分析,拟定水分测量管不同标称容量的容量允差;结果:水分测定管参照流出式分度吸量管进行检定时准确度和不确定度更符合实验需求;结论:为使甲苯法测水分的测定结果更加准确、可靠,应根据水分测定管的生产工艺和检测需求制定出水分测定管的检定规程。

-----英文摘要:---------------------------------------------------------------------------------------

Objective: To suggest capacity allowance of moisture measuring tubes with different nominal capacities. Methods: The capacity allowance of moisture measuring tubes with different nominal capacities was suggested through evaluation and analysis on the measurement uncertainty of the toluene method for moisture determination. Results: The accuracy and uncertainty that were obtained with the moisture measuring tube with reference to efflux indexing pipettes were more aligned with experimental requirements. Conclusion: To ensure the accuracy and reliability of the testing results, we suggest that the standard should lay down vertification regulation of the moisture measuring tube according to production technology and testing requirements of the moisture measuring tube.

-----参考文献:---------------------------------------------------------------------------------------
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[3] ZHONG Li-hong(钟丽红), LIU Ying(刘颖), WANG Wei-jian(王维剑), et al.HPLC evaluation of uncertainty for the determination of cefuroxime reference substance A[J]. Chin J Pharm Anal(药物分析杂志), 2011, 31(11):2191
[4] DU Shu-li(杜书利), ZHANG Zhi-qing(张志清), XIE Jun-yan(谢军燕), et al.Verification Regulation of Working Glass Container(《常用玻璃量器检定规程》JJG196-2006)[S].Beijing(北京):China Metrology Publishing House(中国计量出版社), 2007:17
[5] ZHANG Hong-ya(张红亚), QU Chao-qing(瞿潮庆), XIE Jun-yan(谢军燕), et al.Verification Regulation of Special Glassware(《专用玻璃量器检定规程》JJG10-2005)[S].Beijing(北京):China Metrology Publishing House(中国计量出版社), 2005:3
[6] DU Shu-li(杜书利), ZHANG Zhi-qing(张志清), XIE Jun-yan(谢军燕), et al.Verification Regulation of Working Glass Container(《常用玻璃量器检定规程》JJG196-2006)[S].Beijing(北京):China Metrology Publishing House(中国计量出版社), 2007:8
[7] YE De-pei(叶德培), SHI Chang-yan(施昌彦), JIN Hua-zhang(金华彰), et al.General Terms in Metrology and Their Definitions(《通用计量术语及定义》JJF1001-2011)[S].Beijing(北京):China Zhijian Publishing House(中国质检出版社), 2012:37
[8] CHEN Zhi-hua(陈志华), QIN Zhi-gao(覃志高), HE Shao-ying(何绍映), The advice for the second water checking method in China Pharmacopoeia(methylbenzence method)(对《中国药典》水分测定法中甲苯法的建议)[J].China Pharm (中国药师), 2011, 14(7):1066
[9] LI Yun-long(李云龙), DING Li-xia(丁丽霞), JIN Shao-hong(金少鸿), et al.Standard operating specification of Chinese drug testing(《中国药品检验标准操作规范》)[M].Beijing(北京):China Medical Science Press(中国医药科技出版社), 2010:5

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