GC法测定感冒清热颗粒中胡薄荷酮的含量
GC determination of pulegone in Ganmao Qingre granules
分类号：
出版年·卷·期（页码）：2012,32 (7):0-0
DOI:
10.16155/j.0254-1793.2017.01.01
-----摘要：-------------------------------------------------------------------------------------------
目的: 建立GC法测定感冒清热颗粒中胡薄荷酮的含量。 方法: 色谱柱为FFAP毛细管色谱柱(30 m×0.53 mm×1.0 μm),柱温230℃,FID为检测器,选用乙酸乙酯作提取溶剂。 结果: 胡薄荷酮进样量在0.17~2.73 μg范围内与峰面积线性关系良好(r=0.9999),平均加样回收率(n=6)为97.8%,RSD为1.0%。 结论: 该方法简便、可靠、准确,可用于该制剂的质量控制。
-----英文摘要：---------------------------------------------------------------------------------------
Objective: To establish the determination method of pulegone in Ganmao Qingre granules by GC. Methods: The samples were separated on a column of FFAP(30 m×0.53 mm×1.0 μm),column temperature was 230℃,the FID was used and the ethyl acetate was selected as the extraction agent. Results: The calibration curves showed good linearity in the range of 0.17-2.73 μg(r=0.9999).The average recovery(n=6)was 97.8% with RSD of 1.0%. Conclusion: This method is simple, reliable, accurate and can be used for the quality control of the drug.
-----参考文献：---------------------------------------------------------------------------------------
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