市售西红花药材掺伪染色检测方法的实验研究
Experimental research on the detection methods of Croci Stigma adulteration on the markets
分类号：
出版年·卷·期（页码）：2012,32 (1):0-0
DOI:
10.16155/j.0254-1793.2017.01.01
-----摘要：-------------------------------------------------------------------------------------------
目的: 确认西红花药材中违法染色的色素或染料成分,建立相应的染色成分分析方法。 方法: 采用液相色谱-质谱联用以及对照试剂对照的方法,对染色成分进行鉴定;薄层色谱和高效液相色谱法检测染色物成分。 结果: 西红花药材掺伪染色的主要成分为柠檬黄、胭脂红、金胺O和新品红;对43批市售西红花药材进行了检测,其中32批检测出含有上述4种染色物,存在染色情况。 结论: 建立的检测方法可快速进行西红花药材中掺伪染色的定性检测。
-----英文摘要：---------------------------------------------------------------------------------------
Objective: To identify the pigments or dyes,and establish analysis method for Croci Stigma adulteration. Methods: Using LC-MS method and comparing with the reference regents,to identify the main pigments and dyes.TLC and HPLC analytical methods were used for analysis of Croci Stigma adulteration. Results: Tartrazine,brilliant ponceau,auramine O and new fuchsin were identified as the main pigments and dyes.The results show that the above 4 pigments and dyes could be detected in 32 of totally 43 samples. Conclusion: The established method is able to detect the Croci Stigma adulteration quickly and effectively.
-----参考文献：---------------------------------------------------------------------------------------
[1] ChP(中国药典).2010.Vol Ⅰ(一部):120
[2] Nanjing University of Traditional Chinese Medicine(南京中医药大学).Zhongyao Dacidian(中药大辞典).2nd Ed(第二版).Shanghai(上海):Shanghai Science and Technology Publishers(上海科学技术出版社),2006.3365
[3] ZHANG Jie(章杰).Prohibited dyes and Green dyes(禁用染料和环保型染料).Beijing(北京):Chemical Industry Press(化学工业出版社),2002
[4] RAO Wei-wen(饶伟文),JIANG Ling(蒋玲),ZHAO Chun-yu(赵纯玉),et al.Identification of chemical industry dyes in adulteration of Chinese medicinal materials(几种染色掺假中药的化工染料鉴定).Chin J Pharm Anal(药物分析杂志),2007,27(11):1742
[5] YANG Xin-wei(杨新玮).Dyes(染料).Beijing(北京):Chemical Industry Press(化学工业出版社),2005
欢迎阅读《药物分析杂志》！您是该文第 1997位读者！
