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刊物信息

期刊名称:药物分析杂志
主管单位:中国科学技术协会
主办单位:中国药学会
承办:中国食品药品检定研究院
主编:金少鸿
地址:北京天坛西里2号
邮政编码:100050
电话:010-67012819,67058427
电子邮箱:ywfx@nifdc.org.cn
国际标准刊号:ISSN 0254-1793
国内统一刊号:CN 11-2224/R
邮发代号:2-237
 

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白术茯苓汤不同配比水煎液中多糖的含量研究____

Different proportions of polysaccharide content in Baishu Fuling Decoction.

分类号:
出版年·卷·期(页码):2010,30 (3):0-0
DOI: 10.16155/j.0254-1793.2017.01.01
-----摘要:-------------------------------------------------------------------------------------------

目的 研究白术茯苓汤不同配比水煎液中多糖的含量;方法 水提醇沉法分离出粗多糖,采用蒽酮一硫酸法制得有色糖醛衍生物,用分光光度法进行含量测定。结果 加入4ml、0.3%的硫酸蒽酮溶液,在水浴中加热10min,冷却10min时复方多糖含量测定条件最优。显示627nm处有最大吸收峰,线性关系较好 (r=O.9997),平均回收率为97.33%;结论 白术单煎多糖提取的含量最高,茯苓所占比例越大,含量越低。该方法快速准确、重现性好。

-----英文摘要:---------------------------------------------------------------------------------------

objective To study different proportions of polysaccharide content in Baishu Fuling Decoction. Methods The polysaccharide were extracted with hot water and precipitated with alcohol,The contents of polysaccharide were determined by sulfuric acid-anthrone method by UV spectrophotometry. Result The optimum determination conditions for polysaccbaride contentin in Atractylodes Poria soup were as follows:4 ml 0.3% anthmne-sulfate solution,heating for 20 min in water bath and cooling for 20 min.There is maximum absorption of 627nm peak, good linear relationship (r=0.9997),the average recovery was 97.33%;Conclusion: Atractylodes macrocephala single fry the highest content of polysaccharide extracted, the greater the proportion of Wdfiporia COCos, the lower content. The method is rapid, accurate, reproducible.

-----参考文献:---------------------------------------------------------------------------------------
1 WEN Yue-qiuang(文跃强),PENG Teng(彭腾),JIA BO(贾波)et al. The influence of various extracts Components from Baishu Fuling Decoction to spleen weakness big mouse VIP (白术茯苓汤各萃取部位对脾虚大鼠VIP的影响),Jiangsu J Tradit Chin Med(江苏中医药). 2009, 26(1):14 2 ZHANG Chun(张纯), GUO Wen-biao(郭文彪), WANG Wen-jie(王雯佶) et al. Determination of achyranthis’polysaccharide by the ameliorative sulfuric acid-anthrone colorimetric method(改良蒽酮比色法测定牛膝多糖的含量).Chinese Clinical J C

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