高效液相色谱法测定温胃药酒中肉桂醛的含量___
Determination of Cinnamaldehyde in Wen-wei Yaojiu By HPLC
分类号:
出版年·卷·期(页码):2009,29 (11):0-0
DOI:
10.16155/j.0254-1793.2017.01.01
-----摘要:-------------------------------------------------------------------------------------------
目的:建立高效液相色谱法测定温胃药酒中肉桂醛含量的方法。方法:用十八烷基硅烷键合硅胶为填充剂 ;甲醇-0.5%磷酸(48:52)为流动相; 流速为1.0mL.min-1;检测波长为280nm。结果:均回收率为97.31%,RSD=1.61%。结论: 该方法简便,快速,灵敏,重线性好,可用于该产品质量控制。
-----英文摘要:---------------------------------------------------------------------------------------
Objective:To establish an HPLC method for the determination of Cinnamaldehyde in Wen-weiYaojiu .Methods:The Kromasiltm C18 column was used.The mobile phase was consisted Methanol-0.5% Phosphoric acid (48:52) with 1 mL.min-1 of flow rate,and the detection wavelength was at 280nm. Results:The average recoveries for cinnamaldehyde was 97.31% with RSD of 1.61%.Conclusion:The method is simple,rapid,sensitive and reproducible.The method can be used for quality control.
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