HPLC法测定大黄虫胶囊中大黄酸的含量___
HPLC Determination of Rhein Acid in Capsula Rubarb and Dahuang Zhechong Capsules
分类号:
出版年·卷·期(页码):1998,18 (3):0-0
DOI:
10.16155/j.0254-1793.2017.01.01
-----摘要:-------------------------------------------------------------------------------------------
用高效液相色谱法对大黄虫胶囊中大黄酸进行了含量测定,采用YWG-C18(5μm)4.6mm×250mm色谱柱,以甲醇—水—冰醋酸(330∶170∶5)为流动相,检测波长254nm,柱温40℃,本方法回收率为97.95%,RSD为2.83%,是一种简便、快速、准确的测定方法。
-----英文摘要:---------------------------------------------------------------------------------------
A HPLC method for the determination of rhein acid in Dahuang Zhechong capsules was investigated.The method has been carried out by using the uitrasphere-ODS column and methanol-water-acetic acid as mobile phase.The result showed that this method was simpl
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