国产异戊巴比妥的杂质分离和结构分析___
Study on the Isolation and Structure Determination of a Major Impurity in Domestic Amobarbital
分类号:
出版年·卷·期(页码):1994,14 (2):0-0
DOI:
10.16155/j.0254-1793.2017.01.01
-----摘要:-------------------------------------------------------------------------------------------
本文用高效液相半微量制备柱分离出国产异戊巴比妥中的主要杂质,并用紫外、红外、质谱和氢谱等分析技术进行鉴定,杂质为异戊巴比妥的同分异构体:5-乙基-5-(2-甲基丁基)巴比妥酸。
-----英文摘要:---------------------------------------------------------------------------------------
A major impurity in domestic amobarbital was isolated by HPLC. The impurity structure was elucidated and shown as 5-ethy1-5(2-methylbutyl)-barbituric acid by UV, IR, MS and′ HNMR.
-----参考文献:---------------------------------------------------------------------------------------
欢迎阅读《药物分析杂志》!您是该文第 1131位读者!